- 更多網(wǎng)絡(luò)例句與乙酰乙酸相關(guān)的網(wǎng)絡(luò)例句 [注:此內(nèi)容來源于網(wǎng)絡(luò)欧美熟妇性生活,僅供參考]
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Methods 4-Hydroxy- benzonitrile was treated with sodium hydrogen sulfide and anhydrous magnesium chloride in dimethyl formamide to give thioamide, which was then directly cyclized with ethyl 2-chloroacetoacetate without separation to give ethyl 2-(4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(2) in one-pot; then 2 was formylated with Duff reaction adopting hexamethylenetetramine in trifluoroacetic acid to give ethyl 2-(3-formyl-4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(3); finally, the target compound was obtained by the treatment of 3 with hydroxylamine hydrochloride and sodium formate in formic acid.
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Major procurement of goods: a three-chlorosilanes, dichloromethane, AE activity ester, 3-iodine Silane, special acid, pentyl chloride, triethylamine, thiadiazole, tetrazolylazo acid, 2 - Acetamide, tetrahydrofuran, the four-guanidine, isopropanol, five phosphorus trichloride, sodium vary bitter, acid, sodium phenylacetate, 6-2 silicon n-amine, Ethylacetoacetate , Methyl isobutyl ketone, potassium dihydrogen phosphate, aluminium oxide, DL methionine, N, N-dimethylaniline, NN-diethyl aniline, 4 sodium EDTA, Anhydrous sodium sulfate, ammonium sulfate, potassium sulfate, sodium acetate, sodium carbonate, DMC, formic acid, sodium chloride medicinal, oxalate, protopine, acetone, alcohol, acetic acid, vinegar Ethyl, butyl acetate, methanol, ethanol (anhydrous, industrial, medicinal), formaldehyde, Ye Jian (30%), hydrochloride (industrial-grade, refined grade, reagent level), sulfate (98%), Ammonia, calcium carbonate, chlorine dioxide, 6 - APA ,7-ACA ,7-ADCA ,7-ANCA, sulbactam, ceftazidime activity ester, Deng salt (hydroxymethyl-K, acid precursors Potassium, sodium dihydrogen methyl), resin, the enzyme, water treatment agent, Xiao Mo agent, demulsifier, flocculants, activated carbon, all kinds of medicinal materials, All kinds of additives
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Mission:"equality and mutual benefit, reputation first, unity and cooperation and friendship between the long-term" supply products: ethylenediamine; diethylamide; triethylamine; Diethylenetriamine; three ethylene diamine; three ethylene amines 40; 40 Five ethylene amines; five ethylene amines 6; caprolactam; DMF; allyl amine; N, N dimethylaniline; propylamine; are butylamine; are TOA; 3 Poly Cyanamide; 1,2 c diamine; ethanolamine; diethanolamine, triethanolamine; potassium iodide, potassium hydroxide, potassium permanganate, toluene, xylene, toluene of chlorine ; Acetone, butanone; acetylacetone; ethyl acetate, butyl acetate; Y-butyrolactone; DMC; acetyl of methyl acetate; Sanfu acetyl acid; Sanfu acetyl B Ethyl; methanol, ethanol, isopropanol; propylene glycol; glycerol; propargyl alcohol; 1.3 propylene glycol; xylitol; acetic acid; have acid; mercaptoacetic acid; vary Bitterness; adipic acid; trifluoroacetic acid; oxalic acid, the amino acid; o-amygdalin acid; DL-Acid; anhydrous piperazine; six non-piperazine, furfural, castor oil, ethylene Aldehyde; glutaraldehyde, multi-POM; isopropyl ether; anisole; tetrahydropyrrole; pure pyridine; 1.2 dichloroethane; methylene chloride, chloroform, carbon tetrachloride; hydrazine hydrate; Nonylphenol;-m-cresol; Se phenol; phenol; the tert-butyl phenol; Titanium Dioxide; iron; full Tangfen; Bisphenol A; azo two different nitrile; sodium azide; sodium carbonate ; Sodium chloride; iron oxide; cuprous chloride; thionyl chloride; D4; sodium bicarbonate; ammonia, potassium chloride; anhydrous sodium sulphite; ammonium persulfate; glycol Dingmi; B Glycol ether; calcium chloride; cyclohexanone; cyclohexane, methyl tertiary butyl ether, potassium carbonate, ferric chloride, potassium nitrate; Linsuansanna; zinc oxide; sodium nitrite; antimony oxide; Tartrate; OP-10; TX-10; tablets base; AES; sodium benzoate, sodium citrate; partial sodium silicate, sodium perborate, a sodium carbonate, sodium benzene; Asia sodium chlorate; Wuluo Care products; urea; hydrochloric acid, sulfuric acid, lactic acid; amino acid, hydrogen peroxide, ammonium bicarbonate
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A set of laser monitoring observation system to be used for measure the solubility with a high speed, which is programmed heating apparatus , have designed. The solubility of 1,2-cyclohexanediol were measured in water, methyl acetate, acetic ester, propyl acetate, butyl acetate, methyl acrylate, ethyl acrylate, acetoacetic ester at different temperature.
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objective to determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of edaravone, by gas chromatography.methods sample solution was injected on a gdx column (0.18 mm~0.25 mm) with nitrogen as the carrier gas.the residue was calculated by the external standard method.results the linearity was good over the range of 25 μg/ml~400 μg/ml,with the correlation coefficient of acetone being 0.996 and the average recovery 96.8%.conclusions the method was proved to be simple,rapid,practical and highly sensitive.it is an efficient method for the quality control of acetoacetic ester.
摘要] 目的:用氣相色譜法測定依達拉奉合成起始原料乙酰乙酸乙酯中丙酮的殘留量99久久久精品免费人妖。方法:采用固定相為二乙烯苯乙基乙烯苯型高分子多孔小球(直徑為0.18 mm~0.25 mm)97在线视频免费播放,氮氣為載氣,用外標法測定乙酰乙酸乙酯中殘留丙酮的含量aaa日欧美女。結(jié)果:該方法在丙酮濃度范圍在25 μg/ml~400 μg/ml內(nèi)呈良好的線性關(guān)系亚洲日韩欧美性爱在线,響應(yīng)曲線相關(guān)系數(shù)為0.996,平均回收率為96.8%日本ā片免费观看网站。結(jié)論:本法簡便亚洲四区欧美四区二区三区,快速、實用精品欧美一区二区不卡视频,靈敏度高谁有黄色网址,可有效地用于乙酰乙酸乙酯的質(zhì)量控制。
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Objective To determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of Edaravone, by gas chromatography.Methods Sample solution was injected on a GDX column (0.18 mm~0.25 mm) with nitrogen as the carrier gas.The residue was calculated by the external standard method.
摘要] 目的:用氣相色譜法測定依達拉奉合成起始原料乙酰乙酸乙酯中丙酮的殘留量方法:采用固定相二乙烯苯乙基乙烯苯型高分子孔小球(直徑為0.18 mm~0.25 mm)国产qv,氮氣為載氣欧美一区二区黄色网站,用外標法測定乙酰乙酸乙酯中殘留丙酮的含量视频偷拍网。
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Mission:"equality and mutual benefit, reputation first, unity and cooperation and friendship between the long-term" supply products: ethylenediamine; diethylamide; triethylamine; Diethylenetriamine; three ethylene diamine; three ethylene amines 40; 40 Five ethylene amines; five ethylene amines 6; caprolactam; DMF; allyl amine; N, N dimethylaniline; propylamine; are butylamine; are TOA; 3 Poly Cyanamide; 1,2 c diamine; ethanolamine; diethanolamine, triethanolamine; potassium iodide, potassium hydroxide, potassium permanganate, toluene, xylene, toluene of chlorine ; Acetone, butanone; acetylacetone; ethyl acetate, butyl acetate; Y-butyrolactone; DMC; acetyl of methyl acetate; Sanfu acetyl acid; Sanfu acetyl B Ethyl; methanol, ethanol, isopropanol; propylene glycol; glycerol; propargyl alcohol; 1.3 propylene glycol; xylitol; acetic acid; have acid; mercaptoacetic acid; vary Bitterness; adipic acid; trifluoroacetic acid; oxalic acid, the amino acid; o-amygdalin acid; DL-Acid; anhydrous piperazine; six non-piperazine, furfural, castor oil, ethylene Aldehyde; glutaraldehyde, multi-POM; isopropyl ether; anisole; tetrahydropyrrole; pure pyridine; 1.2 dichloroethane; methylene chloride, chloroform, carbon tetrachloride; hydrazine hydrate; Nonylphenol;-m-cresol; Se phenol; phenol; the tert-butyl phenol; Titanium Dioxide; iron; full Tangfen; Bisphenol A; azo two different nitrile; sodium azide; sodium carbonate ; Sodium chloride; iron oxide; cuprous chloride; thionyl chloride; D4; sodium bicarbonate; ammonia, potassium chloride; anhydrous sodium sulphite; ammonium persulfate; glycol Dingmi; B Glycol ether; calcium chloride; cyclohexanone; cyclohexane, methyl tertiary butyl ether, potassium carbonate, ferric chloride, potassium nitrate; Linsuansanna; zinc oxide; sodium nitrite; antimony oxide; Tartrate; OP-10; TX-10; tablets base; AES; sodium benzoate, sodium citrate; partial sodium silicate, sodium perborate, a sodium carbonate, sodium benzene; Asia sodium chlorate; Wuluo Care products; urea; hydrochloric acid, sulfuric acid, lactic acid; amino acid, hydrogen peroxide, ammonium bicarbonate
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Methods 4-Hydroxy- benzonitrile was treated with sodium hydrogen sulfide and anhydrous magnesium chloride in dimethyl formamide to give thioamide, which was then directly cyclized with ethyl 2-chloroacetoacetate without separation to give ethyl 2-(4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(2) in one-pot; then 2 was formylated with Duff reaction adopting hexamethylenetetramine in trifluoroacetic acid to give ethyl 2-(3-formyl-4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(3); finally, the target compound was obtained by the treatment of 3 with hydroxylamine hydrochloride and sodium formate in formic acid.
采用&一勺燴&方法日韩在线视频台湾,以4-羥基苯甲腈為起始原料,首先與硫氫化鈉和無水氯化鎂在N怎么免费查找黄色网站网址,N-二甲基甲酰胺中反應(yīng)爱搞网,所得中間體不經(jīng)分離,直接加入2-氯乙酰乙酸乙酯進行環(huán)合反應(yīng)久久三区,得到2-(4-羥基)苯基-4-甲基-5-噻唑甲酸乙酯(2)明星黄色视频在线;然后通過六亞甲基四胺/三氟乙酸進行Duff反應(yīng),得到2-(3-甲跖访繟片黄片视频;?4-羥基)苯基-4-甲基-5-噻唑甲酸乙酯(3)91做a免费视频;再經(jīng)鹽酸羥胺/甲酸/甲酸鈉體系脫水得到目標化合物。
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Base played a crucial role in this reaction: in the Pd2/L1 catalyzed α-arylation of ethyl malonate, K3PO4 is the base of choice; in the α-arylation of ethyl acetoacetate, K2CO3 is the most effective base.
在這類催化反應(yīng)中国产毛片小视频,堿的選擇具有重要的影響:以K3PO4為堿视频一区二区红樱桃网站, Pd2/L1催化體系在丙二酸二乙酯的α-芳基化中,富電子溴代芳烴顯示較好的活性日韩视频05; Pd2/L1催化的乙酰乙酸乙酯α-芳基化時精品人人,以 K2CO3為堿,催化體系顯示較好的活性yy6080新觉伦AA午夜视频伊人,這個催化體系可控制反應(yīng)得到α-芳基乙酰乙酸乙酯欧美a日本在线一,而不是脫乙酰基的產(chǎn)物A片AA。
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Base played a crucial role in this reaction: in the Pd2/L1 catalyzed α-arylation of ethy malonate, K3PO4 is the base of choice; in the α-arylation of ethyl acetoacetate, K2CO3 is the most effectiv base.
在這類催化反應(yīng)中91网免费在线观看,堿的選擇具有重要的影響:以K3PO4為堿,Pd2/L1催化體系在丙二酸二乙酯的α-芳基化中在线观看自拍日韩欧美视频网站大全,富電子溴代芳烴顯示較好的活性欧美一级性交网站;Pd2/L1催化的乙酰乙酸乙酯α-芳基化時,以K2CO3為堿,催化體系顯示較好的活性91AV在线观看免费视频,這個催化體系可控制反應(yīng)得到α-芳基乙酰乙酸乙酯国产美女网站在线观看,而不是脫乙酰基的產(chǎn)物大尺度久草。
- 更多網(wǎng)絡(luò)解釋與乙酰乙酸相關(guān)的網(wǎng)絡(luò)解釋 [注:此內(nèi)容來源于網(wǎng)絡(luò)欧美日韩在线亚洲二区综二,僅供參考]
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acetoacetate:乙酰乙酸鹽
acetoacetanilide 乙酰乙酰苯胺 | acetoacetate 乙酰乙酸鹽 | acetoacetic acid 乙酰乙酸
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acetoacetate:乙酰乙酸酯;乙酰乙酸鹽
acetocarmine 醋酸胭脂紅 | acetoacetate 乙酰乙酸酯;乙酰乙酸鹽 | acetoacetate decarboxylase 乙酰乙酸脫羧酶
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acetoacetate decarboxylase:乙酰乙酸脫羧酶
acetocarmine 醋酸胭脂紅 | acetoacetate 乙酰乙酸酯;乙酰乙酸鹽 | acetoacetate decarboxylase 乙酰乙酸脫羧酶
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acetoacetic acid:乙酰乙酸;乙酰醋酸
acetin method 乙酸酯法;醋精法[甘油定量方法] | acetoacetic acid 乙酰乙酸;乙酰醋酸 | acetobutyryl cellulose 乙(酸)丁(酸)纖維素
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acetoacetic acid:乙酰乙酸,乙酰醋酸,丁間酮酸
acetoacetate | 乙酰乙酸 | acetoacetic acid | 乙酰乙酸,乙酰醋酸,丁間酮酸 | acetoacetic ester synthesis | 乙酰乙酸酯合成
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acetoacetic ester:乙酰乙酸酯
acetoacetic acid 乙酰乙酸 | acetoacetic ester 乙酰乙酸酯 | acetoacetic ether 乙酰乙酸乙酯
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acetoacetic ester:乙酰乙酸(乙)酯
acetoacetic acid 乙酰乙酸 | acetoacetic ester 乙酰乙酸(乙)酯 | acetoacetyl-acyl carrier protein 乙酰乙酰-酰基載體蛋白
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ethyl acetoacetic acid:乙基乙酰乙酸
ethyl acetoacetate 乙酰乙酸乙酯 | ethyl acetoacetic acid 乙基乙酰乙酸 | ethyl acetoacetic ester 乙基乙酰乙酸酯
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diacetic ester; ethyl acetoacetate:乙酰乙酸乙酯
乙酰乙酸 diacetic acid; acetoacetic acid | 乙酰乙酸乙酯 diacetic ester; ethyl acetoacetate | 二乙酸甘油酯;甘油二乙酸酯;二乙酰甘油 diacetin; diacetylglycine
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acetoacetic acid amides:乙酰乙酸氨化物
acetoacetic acid 乙酰乙酸 | acetoacetic acid amides 乙酰乙酸氨化物 | acetoacetic acid ester 乙酰乙酸酯