In part one, the reactions of some active fluorine-containing compounds such as 2, 2-dihydropolyfluoroalkanoic acids and ethyl 2-hydropolyfluoroalkenoates were studied and various fluorine-containing heterocyclic compounds were synthesized. Using 2, 2-dihydropolyfluoroalkanoic acids as the starting material, 4-fluoroalkyl quinolin-2-ols, 2- [ -1-hydropolyfluoro-1-alkenyl] -4H-3, 1-benzoxazin-4-ones, 1-aryl -4, 9-dihydro-3-fluoro-alkyl-1H-pyrazo [3, 4-b] quinolin-4-ones, 5-fluoroalkyl-12H-quin olino [2, 1-b] quinazolin-12-ones, 4-fluoroalkyl-1, 3-dihydro-1, 5-benzodiazepin-2-ones and 4-fluoroalkyl-2H-pyrido [1, 2-a] pyrimidin-2-ones were synthesized through its condensation reaction with anilines, anthranilic acid, N'-aryl-o-aminobenzamides, o-nitro aniline, o-amino pyridine and their derivatives and the subsequent transformations. 5-Fluoroalkyl isoxazolidines, 3-fluoro-3-fluoroalkylisoxazolidino [4, 3-c] quinolin-4-ones, 3-fluoroalkylisoxazolino [4, 3-c] quinolin-4-ones and 2-aryl-3per fluoroacylindoles were synthesized by inter-and intramolecular 1, 3-dipolar cycloaddition of fluorine-containing olefins and nitrones.

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METHODS: A model of T cell activation and proliferation was established by stimulated the cells with Con A.T cells were treated with different concentrations of CPT. The expression of CD69, the early marker of CD3(superscript +) T cell activation, was measured by FACS. The proliferation index was determined by carboxyl fluorescin diacetate succinmidyl ester by flow cytometry. The cell-cycle distribution was analyzed by propidium iodide staining.

以ConA刺激小鼠T淋巴細(xì)胞人人看人人上人人干，建立小鼠T淋巴細(xì)胞活化、增殖的模型国产高91亚洲精品福利在线播放，以不同濃度的CPT作用于該模型亚洲精品无码福利在线观看，流式細(xì)胞術(shù)檢測(cè)T細(xì)胞早期活化標(biāo)志CD69分子的表達(dá)；以活體染料羧基熒光素乙酰乙酸染色流式細(xì)胞術(shù)分析CPT在ConA刺激下小鼠淋巴細(xì)胞的增殖相關(guān)指數(shù)一级黄色网站高清无码；以碘化丙啶染色流式細(xì)胞術(shù)分析細(xì)胞周期的分布情況午夜性生活影视。

METHODS: After stimulated with Con A, T cells were treated with different concentrations of TMB-8 alone and its combination with cyclosporine A. The expression of CD69, the early marker of CD3(superscript +) T cell activation, was measured by FACS. The proliferation-related index was determined by carboxyl fluorescin diacetate succinmidyl ester flow cytometry. The cell-cycle distribution was analyzed by propidium iodide staining.

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Methods: A model to evaluate lymphocyte proliferation stimulated with a polyclonal activator, concanavalin A, was established by vital dye carboxyl fluorescin diacetate succinmidyl ester labeling technique. Effects of the different doses of anisomycin on the lymphocyte proliferation were estimated by flow cytometry and MTT methods. The propidium iodide labeling technique was applied to assay the effect of the different doses of anisomycin on changes of the lymphocyte cell-cycle stimulated by ConA or by phorbol ester plus Ionomycin. The percentage of the expression level of CD69 and CD25 on the activated lymphocytes was evaluated by fluorescin-conjugated monoclonal antibody double labeling technique.

以活體染料羧基熒光素乙酰乙酸琥珀酰亞胺酯染色，建立在多克隆刺激劑刀豆蛋白A刺激下評(píng)價(jià)小鼠淋巴細(xì)胞增殖的模型自拍三级青草，通過流式細(xì)胞術(shù)和MTT法分析茴香霉素在不同劑量下對(duì)淋巴細(xì)胞增殖的作用在线青草草永久视频免费播放；采用碘化丙錠染色分析茴香霉素對(duì)ConA或佛波醇酯加離子霉素刺激的小鼠淋巴細(xì)胞周期變化的作用；利用熒光標(biāo)記的單克隆抗體雙染技術(shù)和流式細(xì)胞術(shù)觀察茴香霉素對(duì)小鼠CD3~+T細(xì)胞早期及中期活化標(biāo)志分子CD69和CD25表達(dá)的影響777久久激情久久综合。

Tetrachloroterephthalic acid was prepared by chlorinating terephthalic acid, oleumsolvent and iodine catalyst. Tetrachloroterephthalic acid was acylated by sulphurous oxychloride in the presence of DMF to form tetrachloroterephthaloyl chloride. The acyl chloride product was fluorinated by potassium fluoride and esterified by methanol to synthesize dimethyl tetrafluoroterephthalate. The ester was reduced with potassium borohydride and lithium chloride to give tetrafluoroterephthalyl alcohol. The above product was bromated in the hydrobromic acid to obtain 4-bromomethyl-2,3,5,6-tetrafluoro-benzene methanol. 4-Methyl-2,3,5,-6-tetrafluorobenzene ethanol was obtained by reducing the bromide with magnesium. In the exist of DCC and DMAP, tefluthrin was got by the condensation reaction between 4-methyl-2,3,5,6-tetrafluoro-benzene methanol and-(1RS,3RS)- 3-(2- chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethyl cycolpropanecar-boxylate acid.

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Methods Forty rats were randomized into normal control group and FS group. The normal control group was fed with conventional forage. FS group was fed with dry forage mixed with FS powder for 3 months, the preliminary dose of FS was 200 mgkg^(-1)d^(-1) and then increased progressively by l00 mgkg^(-1)d^(-1) to ensure over half of the rats having diarrhea, and the final dose was 2800 mgkg^(-1)d^(-1). The frequency and amplitude of colic slow wave were detected and the changes of myenteric plexus and ICC were observed by zinc iodide -osmic acid staining method.

方法］SD大鼠40只，隨機(jī)分為2組：正常對(duì)照組湿女孩视频网站、番瀉葉組（飼以含番瀉葉粉的乾飼料鲁鲁A片特级特色黄色影片，起始劑量為200 mgkg^(-1)d^(-1)，以100 mgkg^(-1)d^(-1)劑量遞增十八岁成年网站，保持對(duì)半數(shù)以上動(dòng)物有瀉下作用97精品久久久中文字幕免费，連續(xù)3個(gè)月，終劑量為2800 mgkg^(-1)d^(-1)国产A片色色电影，檢測(cè)大鼠結(jié)腸慢波的頻率及振幅又黄又爽又刺激又色，采用碘化鋅－鋨酸法觀察肌間神經(jīng)叢及ICC變化。

The electric conductivity of solid polyiodides increases largely as the aggrandizement of polyiodide anions"polymerization degree. The solid polyiodides have excellent sterilizing effects and the effect of tetra-n-butyl ammonium undecaiodide is the best of them, and the sterilizing effects increase as the aggrandizement of polyiodide anions" polymerization degree. The sterilizing effects of resinic polyiodides increase as the aggrandizement of polyiodide anions polymerization degree, the heptaiodide resinic polyiodide has better sterilizing effects than the triiodide and pentaiodide.

固體高聚碘系列化合物的電導(dǎo)率隨著高聚碘陰離子聚合度的增加而增加你懂的二区国产，并且增幅較大欧美中文字幕观看；固體高聚碘對(duì)常見細(xì)菌均具有很好的殺滅作用又粗又长的黄A片无码视频，并且隨著高聚碘陰離子聚合度的增加欧美欧美视频a√在线，殺菌能力也隨著增強(qiáng)，其中正四丁基十一碘化銨殺菌劑的效果最佳求可以在线观看的不卡的黄色av网站；樹脂高聚碘隨著高聚碘陰離子聚合度的增加一级少妇A片无，殺菌能力增強(qiáng)看片色色，碘七樹脂高聚碘的殺菌效果要明顯好于碘三樹脂和碘五樹脂高聚碘。

In solid phase process, the polyiodides, which include triiodide, pentaiodide, heptaiodide, nonaiodide and undecaiodide tetra-n-butyl ammonium iodide, tetrabutyl ammonium bromide and tetramethyl ammonium iodide poly-compounds, were synthesized by the low-heat solid phase reaction between iodine and tetra-n-butyl ammonium iodide, tetrabutyl ammonium bromide or tetramethyl ammonium iodide; In complexation process, solution polyiodides were synthesized by complexing action of different agents; In resinifying process, triiodide, pentaiodide, heptaiodide resinic polyiodides were synthesized by ion-exchange when the strong basicity styrene anion exchange resin, potassium iodide and iodine were used as raw materials.

固相法是用正四丁基碘化銨樱花aⅴ一区二区三区四区、四丁基溴化銨或四甲基碘化銨分別與碘作用一道本在视频线高清无码，通過低熱固相反應(yīng)，合成出碘三人人干人人操福利、碘五国产一级无码毛片、碘七、碘九和碘十一形式的正四丁基碘化銨国产av中文字幕、四丁基溴化銨或四甲基碘化銨的系列高聚碘化合物亚洲精品自拍视频网；在絡(luò)合法合成溶液高聚碘的實(shí)驗(yàn)中，選用幾種絡(luò)合劑通過絡(luò)合作用首次合成了溶液高聚碘国产免费永久黄色精品；樹脂法合成高聚碘的實(shí)驗(yàn)是采用強(qiáng)堿性苯乙烯系陰離子交換樹脂一级毛片免费看高清视频在线、碘化鉀和碘為原料，通過離子交換一级毛片免费黄色视频，合成了碘三插操水视频、碘五和碘七形式的樹脂高聚碘。

We found that the iodohydroxylation of 1-2-allenyl selenides with I〓 and water can smoothly proceed in aqueous MeCN at 0℃.

我們發(fā)現(xiàn)在乙腈水溶液中欧美黄色网站址，1www.xx日本黄色视频.com，2-聯(lián)烯基硒醚可以和碘發(fā)生羥碘化作用，碘和羥基高度區(qū)域和立體選擇性加成到1激情.com，2-聯(lián)烯基硒醚的β黄色网站免费看看，γ-位。

Copper iodide CuI has a apparent inhibition effect on addition rearrange of the Grignard reagent with carbonyl compounds.

為抑制烯丙基格氏試劑與羰基化合物加成反應(yīng)中的重排反應(yīng)可以看性爱视频的网站，進(jìn)行了碘化亞銅CuI對(duì)此類格氏試劑及加成產(chǎn)物組分比例關(guān)系的研究正在播放麻豆国产AV，CuI對(duì)這類化合物加成反應(yīng)重排有明顯的抑制作用。

iodation：碘化作用

iodate碘酸鹽 | iodation碘化作用 | iodic碘的

ethanoyl iodide：乙酰碘

ethanoyl chloride乙酰氯 | ethanoyl iodide乙酰碘 | ethanoylation乙跞毡拘园豢ǎ化<作用>

iodination：碘化作用

iodide 碘化物 | iodination 碘化作用 | iodine number 碘值

iodization：碘化作用

iodization碘化作用 | iodize加碘;碘化 | iodizedstarch碘化淀粉

iodization：加碘化物(作用)

亞碘酸鹽 iodite | 加碘化物(作用) iodization | 碘化淀粉 iodized starch

iodinated casein; iodocasein：碘化酪蛋白

碘化酶 iodinase | 碘化酪蛋白 iodinated casein; iodocasein | 碘化(作用) iodination

.cl：清除率

藥-時(shí)曲線下面積(AUC)最小,是碘油組的80%,清除率(CL)高于碘油組和化療組(P<0.05). 表明白芨膠有較好的緩釋作用,且其作用強(qiáng)于碘化油. 黎維勇等[5]研究了氟尿嘧啶白芨微球?qū)υl(fā)性肝癌患者肝動(dòng)脈栓塞后的體內(nèi)藥代動(dòng)力學(xué)過程,