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The results show that:(1) after MA for 20h, single phase bcc nanocrystalline supersaturate solid solution formed in Fe84Nb7B9 and Fe80Ti8B12 alloys; the thermal stability of nanocrystalline microstructure in Fe80Ti8B12 alloy was improved significantly than that in Fe84Nb7B9 alloy, and the decomposition temperature of supersaturate solid solution decreased in Fe80Ti8B12 alloy.(2) under 30MPa/900℃/0.5h hot-press sintering conditions, the relative density of Fe84Nb7B9 and Fe80Ti8B12 bulk alloys were 96.7% and 95.5%, respectively. Compared with Fe84Nb7B9 alloy (muti-phase microstructure), Fe80Ti8B12 alloy was composed of superfine crystalline (50~200nm) of single phase α-Fe;(3) the magnetic properties of Fe80Ti8B12 bulk alloy σ(subscript s=198.6emu/g, H=54.6Oe were more excellent than that of Fe84Nb7B9 bulk alloy σ(subscript s=162.9emu/g, H=105.1G, it was related to the different phases formed during hot-press sintering and the grain size of nanocrystalline powder.

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Moreover, the hot compressive deformation behavior of the RS/PM AZ91 magnesium alloy and AZ91 alloy matrix composite were also investigated, the conclusions are drawn as follows:1. The processing parameters of the atomization-twin rolls quenching technology were optimized as follows: the diameter of the nozzle 1mm, the wheel velocity 25m/s, the pressure of atomization gas 0.3MPa and Ar gas for melt injection 0.1MPa. The RS AZ91 alloy flakes exhibited fine and uniform microstructures. When the flakes were extruded at 673K, extruded velocity of 0.1mm/min and extrusion ratio of 25:1,the magnesium alloy rods with clean surface, uniform dimension and excellent mechanical properties were obtained.2. The RS AZ91 magnesium alloy powders prepared by atomization-twin rolls quenched technology exhibited fine equiaxed grains with the grain size of 1-3μm, the phase constituent included supersaturate solid solution phaseα-Mg and miner fineβ-Mg_(17)Al_(12) phase. The as-extruded materials also exhibited equiaxed grains with the size of 5-7μm and a large number of fineβ-Al_(12)Mg_(17) and fewer AlMg_2Zn phases were detected in the alloy.

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Electrochemical measurements of the singler A2B7 and A5B19 phase alloy showed that, the activation properties of singler type A2B7 and AsB19 phase composition alloys were the same. The maximum discharge capacity (386.12mAh/g) of A2B7 type phase alloy was slightly higher than the maximum discharge capacity (371.38mAh/g) of A5B19 type phase alloy. The cyclic stability of alloy electrode of both A2B7 and A5B19-type phase alloy were all very well. The capacity retention rate of 100 cyclic was more than 85%.The high-rate discharge (HRD900=85%) of AsB19phase alloy was higher than the high-rate discharge (HRD900=76.6%) of A2B7phase alloy.

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The results show that Fe0.13[Co20Ni80]0.87 alloy fibers are characterized with thin diameters between 0.3 and 2.0 μm, with high aspect ratio, dense and smooth surfaces. The crystalline size of the alloy fibers are mainly influenced by the thermal reduction temperature and are in the range of 20 to 50 nm with a corresponding reduction temperature range of 300 to 700 ℃. The magnetic properties of the alloy fibers are largely affected by the carbon content and crystalline sizes of the alloy fibers. With increasing thermal reduction temperature, the coercivity decreases while the saturation magnetisation value of the alloy fibers dramatically increases at lower reduction temperatures. The alloy fibers prepared at reduction temperature of 700 ℃ have a saturation magnetisation value of 120 Am2/kg and a coercivity value of 10.4 kA/m, respectively.

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The results show that the dissolution process of prefabricating alloy can be divided into two periods when the temperature of zinc melt is below the melting point of aluminum.Firstly,zinc melts infiltrates into the prefabricating alloy and then Zn-Al-TiC alloy forms in the surface layer of the prefabricating alloy.Secondly,the Zn-Al-TiC alloy of this alloy surface layer begins to dissolve to the zinc melt.

結(jié)果表明：當鋅熔體溫度低于鋁熔點時，預(yù)制合金的溶解可分為兩個階段：第一階段為液態(tài)鋅向預(yù)制合金中浸滲久久视频一二区，并在預(yù)制合金表層內(nèi)形成Zn-Al-TiC合金精品久久九九九久久久久国产；第二階段為預(yù)制合金表層內(nèi)的Zn-Al-TiC合金開始溶解并進入鋅熔體。

At 1273K, the density of dislocations were considerably decreased in deformed TiAlMnNb alloy, twinning and 11 superdislocations were hardly observed, but few 1/212 superdislocations and 01 perfect dislocations were found in deformed TiAlMnNb alloy. In high temperature range, brittle-to ductile transition had already occurred in deformed TiAlMnNb alloy, unpinning and climbing were the dominant deformation behavior in TiAlMnNb alloy. In the same way as TiAlMnNb alloy, different distinguishing feature the dislocation configuration at low, intermediate and high temperatures emerged in deformed TiAlMnNbB alloy.

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