In this thesis, the research about surface modification of titanium alloy was carried on starting with improving stability of calcium phosphate biomedical coating by force of chemical treatment, Physical Vapor Deposition of titanium metal at high temperature and Electrophoresis Codeposition and sintering technology of the coating. By way of the studying of graded design of microstructure and composition of coating and EPCD and sintering technology, a systemic technology by which a calcium phosphate graded ceramic coating was prepared and sintered rapidly on the surface of a complex shaped product was obtainedand a high function titanium alloy/bioglass/hydroxyapatitegraded coating wasdeveloped.

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Employing high-dilute method and 5-fold excess amine prepared two new "two-armed" acyclic diamine intermediates I_a and I_b, which are also intermediates of synthesizing microcyclic compounds, and eight aromatic Schiff bases, II_, were synthesized from reaction of I_a or I_b condensing with different aromatic aldehydes. Their composition and structure were characterized by Elemental analysis, IR, UV-Vis, LIF,~1HNMR and MS. The hydrogen bond interactions and MS fragmental patterns were also discussed.3. Several novel transition metal complexes using II_a as ligand were synthesized and identified by Elemental analysis, IR, UV-Vis,~1HNMR and molar conductivity.

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