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The stability of isophorone disocyanate and the affecting factors of in-situ miniemulsion polymerization have been studied to carry out the simutaneous or two-step procesure of polyaddition and radical polymerization.

本文主要研究了水敏性單體IPDI的穩(wěn)定性和原位細乳液聚合規(guī)律，探索在細乳液中分步或同步實現(xiàn)縮聚反應(yīng)與自由基聚合的新方法久久人人操，提出了水敏性單體的細乳液聚合實施方法91在线人人艹。

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Parameters in the kinetical equation have been work out. Decomposition reaction of MnCO〓 is followed the shrinking core model, and the control step is chemical reaction.

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A one-pot chemoselective reduction and lactonization of(4S,5R)-hemiesters was carried out to afford high-yielding(3aS,6aR)-lactone,a key chiral building block for the biotin synthesis. One-step introduction of carboxybutyl chain onto(3aS,6aR)-thiolactone was reached upon treatment of zinc reagent 25 in the presence of nanopalladium via an improved Fukuyama coupling under mild reaction conditions.

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By use of titration analysis, the thesis investigated various factors such as isocyanate, PE molecular weight, reacting substance molecular ratio, reacting temperature and time etc. influencing upon prepolymerization step. It was found that 2, 4-tolulene diisocyanate and 4, 4'diphenylmethane diisocyanate is more rapidly reacted with PE600 than HDI. With PE molecular weight increasing, the reacting temperature or time should be raised or extended relevantly. Thus PE2000+2HDI pre-polymerization should be better carried out under some catalyst, for example, Triethylene diamine , Dibutyltin dilaurate and Tin octoate were used.

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In this article, star-high vinyl content polybutadiene was prepared using a multi-functional organolithium anionic initiator by " one-step " process. On the basis of 250ml glassware experiment ,we improved the experiment in 2L metal kettle. The polymerization condition was got as follows: polymerization temperature : 50-60 ℃, monomer content : 8-llg/100ml, polymerization time : 3~4 hours.Chracterizations were carried out by 'H-NMR, IR and GPC.

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