The method is characterized in that:(1) the reflux of the 2-[N, N- 2amino]-3-cyano-group-4-thiopheneacetic-5-carboxylic acid tetra ester is carried out in the proper sodium hydroxide aqueous solution of alcohol for 5h to 6h and the pH value is kept over 10 during hydrolysis;(2) the ethanol of 20 per cent to 60 per cent is added and then the strontium chloride aqueous solution with 2times to 2.5times molal weight is directly added, precipitates the crystal, is filtered and dried;(3) water is added to carry out the reflux and the little salt packed in the crude product is removed, and the product is collected through heat filtration.

其特征在于：①將2--3-氰基-4-羧甲基噻吩-5-羧酸四酯在適量氫氧化鈉水醇溶液中回流5～6小時(shí)欧美爆乳激情A片，水解過(guò)程保持pH值10以上；②然后再加入20-60％乙醇人人干日日爱，隨后直接加入2-2.5倍摩爾量氯化鍶水溶液国内精品盗摄系列，析出結(jié)晶，過(guò)濾全色黄大色大片免费久久老太黄色片，晾干色色色爽爽爽；③加水回流，除去粗品中包裹少量鹽农村老妇乱子伦视频，熱過(guò)濾黄网站色成年大片大免费，收集產(chǎn)品。

Furthermore, influences of different phosphate salts at various concentrations on the ionization efficiency of phosphopeptide were investigated systematically, finding that the signal intensity for phosphopeptide 48FQEEQQQTEDELQDK63 digested from β-casein were 5 to 8 times increased in an optimized condition with 10 mmol/L ammonium monobasic phosphate or 3 to 4 times increased with 10 mmol/L ammonium dibasic phosphate as additive to matrix 2,5-dihydroxybenzoic acid, respectively.

考察了兩種適合于磷酸化肽離子化的基質(zhì)類(lèi)型2性a免费视频\，5-二羥基苯甲酸和2欧美日韩www.59要艹，4，6-三羥基苯乙酮717午夜福利视频网。用2国产AV天天更新，5-二羥基苯甲酸作為基質(zhì)時(shí)，當(dāng)加入10 mM 磷酸氫二銨時(shí)，磷酸化蛋白質(zhì)β-casein的磷酸肽 48FQEEQQQTEDELQDK63的離子化效率可以增強(qiáng)5-8倍黄色片欧美性爱，當(dāng)加入10 mM磷酸二氫胺時(shí)久久e6精品视频，磷酸肽的離子化效率可以增強(qiáng)3-4倍。

The results showed that monocarboxylic acid stearic acid played a role of surfactant, and the product was still orthorhombic Ce2O(CO3)2·H2O with a high crystallization degree. In turn, duality-carboxylic acid tartaric acid...

實(shí)驗(yàn)結(jié)果表明在尿素及硝酸鈰的混合溶液中分別加入一元羧酸硬脂酸三级性爱视频免费在线观看，二元羧酸酒石酸和三元羧酸檸檬酸時(shí)18网站在线免费，一元羧酸硬脂酸在混合溶液中只起表面活性劑的作用，其產(chǎn)物為斜方晶系的單晶Ce2O(CO3)2.H2O微粉好看黄色视频，且表面活性劑硬脂酸的加入使得晶體的晶化程度明顯提高人人射人人摸人人草人人操人人射；而二元羧酸酒石酸與三元羧酸檸檬酸在均相反應(yīng)中則起螯合劑的作用，分別與Ce3+形成螯合物酒石酸鈰和檸檬酸鈰色网站五月天，這些結(jié)果的造成是由于其反應(yīng)機(jī)理的不同所導(dǎo)致的91狠狠综合久久久久精品网站。

Methods: M-CSF-dependent bone marrow cells were isolated from 5-6 weeks old mice, and cultured in the presence of MCSF (25μg/L) with different concentrations of TNF-α(0, 1, 10, 100 μg/L) for 5 days, the formation of TRAP multinucleated cells was observed. These cells were also cultured in the presence of both RANKL (30 μg/L) and M-CSF (25 μg/L) with or without 10 μg/L TNF-α for4, 5, 6 and 9 days. The number of TRAP multinucleated cells and resorption pits on dentine slices were counted under light microscope.

選用小鼠巨噬細(xì)胞集落刺激因子依賴性非附著性骨髓細(xì)胞，在含有25μg/L M-CSF和0国产精品综合色区日韩，1网色网站大全cao，10，100μg/L TNF-α的α-MEM培養(yǎng)液中培養(yǎng)5d后国产一区鲁鲁在线视频免费播放，觀察抗酒石酸酸性磷酸酶染色陽(yáng)性多核細(xì)胞的形成老牛影视无码av一区；細(xì)胞在含有25μg/L M-CSF和30μg/L sRANKL的α-MEM培養(yǎng)液中進(jìn)行培養(yǎng)，比較加入和不加入10μg/L TNF-α培養(yǎng)4一级黄色视频。、5国产乱子精品的A片视频、6和9d后，所形成的TRAP多核細(xì)胞的數(shù)目和骨吸收面積经典自拍视频欧美日韩在线观看网站。

Methods: M-CSF-dependent bone marrow cells were isolated from 5-6 weeks old mice, and cultured in the presence of M-CSF (25 μg/L) with different concentrations of TNF-α(0, 1, 10, 100 μg/L) for 5 days, the formation of TRAP multinucleated cells was observed.

選用小鼠巨噬細(xì)胞集落刺激因子依賴性非附著性骨髓細(xì)胞1024在线视频一区二区精99，在含有25μg/LM-CSF和0，1国模精品一区，1091POPNY老北熟女，100μg/LTNF-α的α-MEM培養(yǎng)液中培養(yǎng)5d后，觀察抗酒石酸酸性磷酸酶染色陽(yáng)性多核細(xì)胞的形成黄片欧美日韩一片二片三片；細(xì)胞在含有25μg/LM-CSF和30μg/LsRANKL的α-MEM培養(yǎng)液中進(jìn)行培養(yǎng)九九色影院亚洲欧洲，比較加入和不加入10μg/LTNF-α培養(yǎng)4、5国产一级性生活免费视频、6和9d后黄色黄片，所形成的TRAP多核細(xì)胞的數(shù)目和骨吸收面積。

Methods 100 cases were randomized into treatment group in which 50 cases were treated with Safflower injection via carotid artery infusion, added Safflower injection 20ml into 0.9% sodium chloride injection 60ml with the 4ml/min velocity, once a day; control group in which 50 cases were treated with venous drip of Safflower injection, added Safflower injection 20ml into 0.9% sodium chloride injection 500ml. After therapy, the curative effect啦啦啦www观看在线下载、 myodynamia and hemorrheology were compared between the two groups.

將100例腦梗死患者隨機(jī)分為紅花注射液頸動(dòng)脈灌注組50例和紅花注射液靜脈滴注組50例人人欧美乱码专区视频免费，治療組：于0.9%氯化鈉注射液60ml中加入紅花注射液20ml，以4ml/min的滴速經(jīng)頸動(dòng)脈灌注超碰123；對(duì)照組：以紅花注射液20ml加入0.9%氯化鈉注射液500ml中靜滴理论片网址，20天后對(duì)兩組療效進(jìn)行分析并觀察治療前后肢體肌力及血液流變學(xué)變化一区二区免费看的黄色片子。

Objective To observe the clinical efficacy of treatment in acute cerebral infarction by Safflower injection via carotid artery infusion.Methods 100cases were randomized into treatment group in which50cases were treated with Safflower injection via carotid artery infusion,added Safflower injection20ml into0.9%sodium chloride injection60ml with the4ml/min velocity,once a day;control group in which50cases were treated with venous drip of Safflower injection,added Safflower injection20ml into0.9%sodium chloride injection500ml.After therapy,the curative effect、myodynamia and hemorrheology were compared between the two groups.

目的 探討頸動(dòng)脈灌注紅花注射液治療急性腦梗死的臨床療效方法將100例腦梗死患者隨機(jī)分紅花注射液頸動(dòng)脈灌注組50例和紅花注射液靜脈滴注組50例性插图真人无遮挡，治療組：于0.9%氯化鈉注射液60ml中加入紅花注射液20ml人妻基地，以4ml/min的滴速經(jīng)頸動(dòng)脈灌注；對(duì)照組：以紅花注射液20ml加入0.9%氯化鈉注射液500ml中靜滴甜蜜蜜手机在线观看，20天后對(duì)兩組療效進(jìn)行分析并觀察治療后肢體肌力及血液流變學(xué)變化。

METHODS: Cultured THP-1 monocytes were induced to macrophages by 0.1 μmol/L phorbol myristate acetate, and the differentiated THP-1 macrophages were incubated with 200 μmol/L Hcy for 24, 48 and 72 hours respectively. Then cell supernatant and lysate were collected as condition medium.

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In addition, mRNA expression of ANF was abolished by sodium nitroprusside, an exogenous NO donor.

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In the hydroxylation of phenol with H〓O〓 in the presence of Ti-ZSM-5, water is best solvent. It produces catechol and hydroquinone simultaneously, and catechol/hydroquinone ratio is approximately 0.85. The results show H〓O〓 utilization ratio increase 14%, when nonoxidizable weak acid HAc is added into the reaction system. Under the conditions of Ti-ZSM-5 as catalyst, phenol/H〓O〓 ratio being 10, a little HAc, temperature 75℃, reaction time 6h, H〓O〓 utilization ratio reaches 74. 6mo1% in the reaction.

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