The Diels-Alder cycloadditions of [60] fullerene for preparation of optical limitingmaterials are discussed in chapter 3 and 6. Soluble cycloaddition derivatives of 〓aresynthesized by the reaction of 〓 with indene,1,1'-biindene andcyclopentadiene derivatives.〓Particular, the Diels-Alder cycloaddition of 〓 with1,1'-biindene under controlled conditions affords the stable monoadduct 〓〓of novel structure, which was confirmed by HPLC, FTIR, FD-MS,〓NMR,〓 NMR, HMQC and HMBC spectra, Its two bridgehead cage carbons resonate at70.91ppm, The 〓 NMR spectra showed 38 lines consistent with the 〓 symmetryassociated with [6,6] addition. The 〓 shows similar optical limitingproperties to that of 〓 in toluene for 8ns laser at wave length 532nm. Moreover, thehigh solubility of this adduct in polar solvents such as THF, acetone enables itsincorporation into sol-gel glass matrix. The thin films prepared via the sol-gel methodshow improved OL behaviour compared to those of 〓. The langmuir-Blodgett filmformation and uv-visible absorption of 〓 are also investigated. LBmonolayer of this compound is prepared on the air-water interface at 〓 mol/l. In chapter 4, three water-soluble derivatives of [60] fullerene: fullerol(1), theaddition product (2)of fullerol (1)with polyvinylpyrrolidone and fumaric acidderivative of 〓(3) are synthesized and characterized.

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By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

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The works exhibited this time is the production under this thinking. I will not limit myself in such an abstract or traditional label. The direct or indirect calligraphy, Taiji, sculpture, poem and philosophy, aesthetic thoughts absorbed from paintings allow me to realize that the form of paintings is not just a key problem, no one shall find the freedom exit as when Duchamp's works were completely destroyed. And there is no one who is as frank and smart as Picasso to change the form game into the local snack. In some history phases, a kind of thinking ways and a kind of language styles may gain the upper hand. But comparing to stable accumulation of the history of culture and aesthetic, the pure quality of painting spirant will forever be an important premise of painting criticism.

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Part four, the author gives some advice of perfecting the system of Chinese Counterclaim, which is the important part in the paper .In this part, the author introduces the system of counterclaim in other countries and makes comparison with Chinese counterclaim. On the basis of comparison, the author concludes that we should absorb the advantages of the two law system and perfect Chinese counterclaim from four aspects. That is to say prefect the premise for accusation, divide the compellent counterclaim and discretionary counterclaim, the instance for counter-counterclaim, the trial of claim and counterclaim and so on.

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With the analysis and discussion of their photoini- liability, it was indicated that their max are all around 330 nm, and all of them have excellent solubility in water and good photoinitiability. Furthermore, the three Photoinitiators with α-tert-amine are obviously superior to the one with just α-sec-amine. Among the four photoinitiators l-(4-aminophenyl)-2-diethylamino-l- propanone dihydrochloride is the best and it has excellent use value.

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For frequency information fluid identification technology:the basic theory of fluid identification based on frequency information has been introduced,for inner and external factor affecting frequency,some steps have been proposed to attain reserved amplitude and frequency analysis data with high resolution,high S/N ratio;through the comparison of time-frequency analysis method, the high accuracy time-frequency analysis method has been selected to extract time-frequency attributes;the analysis method flow of common single frequency fluid identification has been proposed,according to the data of full frequency band,several anomaly zone modes of common single frequency attribute have segregated; incorporating converted wave and compression wave,fluid identification method based on PS wave combined time-frequency analysis has been proposed;the AVO property of various fluid type in frequency domain has been studied;the generalized fourier analysis method,Proni absorption filter has been introduced,and researched for anti-noise and for the seismic processing interpretation flow.The above technology have been applied to fluid identification of organic reef in WBT area in the east of Sichuan and fluid identification of clastic rock in GUANGAN area in the middle of Sichuan,the results show that the above methods are effective.

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Ma Yuan admires the great artists of the pre-Renaissance very ,mucn,sucn as ,poteqilli,Angelica,and Masaqeu,etc,The art of these artists lied in the period between theMiddla Ages and the Renaissance,during which the divine spirit of the Middle Ages was finely inherited,and the spitrit and breath ofa neew age was gradually standing out.

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The results show that the as-synthesized chalcone-containing copolymers are a kind of thermosensitive polymer with a lower critic solution temperature and the LCST of the copolymer decreases with the increase of the chalcone content in the copolymer. With the increase of the solvent polarity, both the maximum absorption wavelength and the fluorescence emitting wavelength of the chalcone-containing copolymers redshifts, and the intensity of fluorescence first increases, then decreases, which exhibits solvent polarity sensitive fluorescence properties.

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