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In the determination of methyl acrylate,butyl acrylate and methyl methacrylate in ambient air,the sample was absorbed with active carbon and resolved with carbon bisulfide,and then determined by GC.After the qulitation by retention time and quantitation by external standard method,the good linearity and low detection limit were got.

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The potential windows in acidic, neutral or alkaline medium were respectively 4.4 V, 4.0 V and 3.0 V. In the electrolyte including Ferri/Ferrocyanide, the electrode surface kept good activity, and the electrochemical reaction occurring on the surface was a diffusion-controlled reaction, with good quasi-reversibility.

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